%0 Journal Article
%4 dpi.inpe.br/plutao/2012/06.21.19.30.58
%2 dpi.inpe.br/plutao/2012/06.21.19.30.59
%@doi 10.1149/1.4704954
%@issn 1938-5862
%F lattes: 3838039471471060 3 SaitoSouAzeFerBal:2012:ElDeRe
%T Electrochemical determination of the real area of nanocrystalline boron doped diamond
%D 2012
%A Saito, Eduardo,
%A Souza, Fernando A.,
%A Azevedo, Adriana Faria,
%A Ferreira, Neidenêi G.,
%A Baldan, M. R.,
%@affiliation
%@affiliation
%@affiliation Instituto Nacional de Pesquisas Espaciais (INPE)
%@affiliation Instituto Nacional de Pesquisas Espaciais (INPE)
%@affiliation Instituto Nacional de Pesquisas Espaciais (INPE)
%@electronicmailaddress
%@electronicmailaddress
%@electronicmailaddress adriana@las.inpe.br
%B ECS Transactions
%V 43
%N 1
%P 169-176
%X The present work is devoted to evaluate the area of samples of nanocrystalline Boron Doped Diamond grown with different dopant solutions. The samples were characterized by Scanning Electron Microscopy (SEM) and Atomic Force Micrsocopy (AFM) and electrochemically by Differential-capacitance (Mott-Schottky plots) and Cyclic Voltammetry. By SEM was possible detect "cauli flower" morphology and by AFM was possible to quantify the roughness of the samples. We evaluate the dopant level by Raman spectroscopy and by Mott Schottky plots. The electrochemical roughness measured by AFM was compared with the roughness determined Cyclic Voltammetry.
%@language en
%3 ECS Trans.-2012-Saito-169-76.pdf